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β型四钼酸铵的制备及结晶过程

吴争平 尹周澜 陈启元 张平民

中南工业大学学报(自然科学版)2001,Vol.32Issue(2):134-138,5.
中南工业大学学报(自然科学版)2001,Vol.32Issue(2):134-138,5.

β型四钼酸铵的制备及结晶过程

The preparation of ammonium β-tetramolybdate and the crystallization process

吴争平 1尹周澜 1陈启元 1张平民1

作者信息

  • 1. 中南大学化学化工学院,
  • 折叠

摘要

Abstract

The ammonium β-tetramolybdate was prepared and the preparing process included two courses: preparing ammonium tetramolybdate by the method of acidified deposition; and preparing ammonium β-tetramolybdate by the method of seeded decomposition. The second course included two processes: one was born of crystal seeds(pH=1.2), the other was growth of crystal seeds(pH=2~3). The TGA and DTA proved that the crystal was ammonium α-tetramolybdate prepared by the method of acidified deposition and was ammonium β- tetramolybdate prepared by the method of seeded decomposition. The thermodynamics and the dynamics of the process were analyzed. The mechanism of crystallization process and the control of the crystalline were discussed simply in this paper.

关键词

四钼酸铵/结晶/热力学分析/动力学分析

分类

化学化工

引用本文复制引用

吴争平,尹周澜,陈启元,张平民..β型四钼酸铵的制备及结晶过程[J].中南工业大学学报(自然科学版),2001,32(2):134-138,5.

中南工业大学学报(自然科学版)

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