天津科技大学学报2004，Vol.19Issue(z2)：141-144,4.
ANALYSIS OF PENTACHLOROPHENOL IN WATER BY PURGE AND TRAP CONCENTRATOR COUPLED TOGAS CHROMATOGRAPHY
ANALYSIS OF PENTACHLOROPHENOL IN WATER BY PURGE AND TRAP CONCENTRATOR COUPLED TOGAS CHROMATOGRAPHY
Huixia Lan 1Yuancai Chen 1Zhonghao Chen1
作者信息
- 1. Paper making & pulping control engineering research center, South China University of Technology,Guangzhou 510640, China
- 折叠
摘要
Abstract
It is convenient and time saving to analyze pentachlorophenol (PCP) in water by purge and trap concentrator coupled to gas chromatography that avoids employing a great deal of organic solvent: In this paper, the appropriate purge and trap conditions of PCP are determined: the trapped sorbent is TenaxGC; the purge gas is pure nitrogen and purge flow is 40ml/min; the purge time is 30min. A series of standard PCP water samples 5, 10, 50, 100, 200,400, 800, 1000ppb are analyzed in order to obtain standard curve, and the linear regressive equation obtained is Y=109.65X-687.72, which correlation coefficient r is 0.9949. The precision of the method is determined with 0.5ppb PCP water sample, and the standard deviation measured is 3%. The detection limit for PCP is 0.2ppb.关键词
purge and trap concentrator/gas chromatography/pentachlorophenolKey words
purge and trap concentrator/gas chromatography/pentachlorophenol分类
轻工纺织引用本文复制引用
Huixia Lan,Yuancai Chen ,Zhonghao Chen..ANALYSIS OF PENTACHLOROPHENOL IN WATER BY PURGE AND TRAP CONCENTRATOR COUPLED TOGAS CHROMATOGRAPHY[J].天津科技大学学报,2004,19(z2):141-144,4.
