分析化学2001，Vol.29Issue(2)：158-160,3.
顶空固相微萃取-气相色谱表面发射火焰光度检测法测定底泥中的丁基锡化合物
Determination of Butyltin Compounds in Sediments by Headspace Solid Phase Microextraction and Capillary Gas Chromatography with Flame Photometric Detector Using Quartz Surface-Induced Luminescence
摘要
Abstract
Solid phase microextraction(SPME) can be effectively used to extract volatile and semivoltaile organic compounds from different environmental matrix. In this paper, we utilize headspace-SPME technique combined with capillary gas chromatography (CGC) and a laboratory modified flame photometric detector using quartz surfaceinduced luminescence (QSIL-FPD) for analyzing butyltin compounds in sediments. The detection limits of mono-,di-, and tri-butyltin compounds, based on the signal equal to 3 times the baseline noise are 16.9 ng/g, 1.58 ng/g adn 0.17 ng/g, respectively.关键词
固相微萃取/毛细管气相色谱-表面发射火焰光度检测器/丁基锡分类
化学化工引用本文复制引用
刘稷燕,江桂斌..顶空固相微萃取-气相色谱表面发射火焰光度检测法测定底泥中的丁基锡化合物[J].分析化学,2001,29(2):158-160,3.基金项目
本文系国家自然科学基金 （）
