分析测试学报2000，Vol.19Issue(2)：1-7,7.
用C60键合硅胶固定相液相色谱分离杯芳烃及杯芳冠醚类化合物
Separation of Calixarenes and Calixcrowns with a C60 Bonded Silica Stationary Phase in Normal _ Phase Liquid Chromatography
摘要
Abstract
Separations of calixarenes and calixcrowns have been investigated on self made C60 bonded silica phase with isopropanol cyclohexane, chloroform－cyclohexane and dichloromethane－cyclohexane as mobile phase. The retention of the calixarenes and calixcrowns decreased with increasing the content of polar solvent in the mobile phase. Of the three polar solvents, isopropanol was found to be the strongest solvent for elution of the calixarenes and calixcrowns on the C60 bonded silica. The separation selectivity of the C60 bonded silica stationary phase for the calixarenes and calixcrowns was depended on the polar solvents. A good separation of the calixarenes and calixcrowns on the C60 bonded silica stationary phase was achieved by using an appropriate mobile phase.关键词
高效液相色谱法/硅胶/固定相/杯芳烃/杯芳冠醚/富勒烯Key words
HPLC/Silica/Stationary phase/Calixarene/Calixcrown/Fullerene分类
化学化工引用本文复制引用
冯钰,胡玉玲,李建森,刘英,达世禄,陈远荫..用C60键合硅胶固定相液相色谱分离杯芳烃及杯芳冠醚类化合物[J].分析测试学报,2000,19(2):1-7,7.基金项目
国家自然科学基金资助项目(29875020) （29875020）
留学回国人员资助基金项目 （）
