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耐高温强碱有机硅消泡剂的研制

陈晓军 包宗宏 陶刚 周邢

日用化学工业2009,Vol.39Issue(4):230-233,237,5.
日用化学工业2009,Vol.39Issue(4):230-233,237,5.

耐高温强碱有机硅消泡剂的研制

Preparation of silicone defoamer resisting to high temperature and strong alkali

陈晓军 1包宗宏 1陶刚 1周邢1

作者信息

  • 1. 南京工业大学,化学化工学院,江苏,南京,210009
  • 折叠

摘要

Abstract

Starting from preparation of silicone defoaming surfactant, conditions that affect the foam inhibiting performance were determined through single-factor and L16(45) orthogonal experiments. The optimal synthesis process conditions were identified as:mass ratio of methyl silicone oil to hydroxyl silicone oil 4:1 ;MQ silicone resin mass fraction 10% ;mole ratio of Me3SiO0.5 to SiO4/2 of MQ silicone resin 0.8;hydrophobic silica mass fraction 8% ; potassium hydroxide mass fraction 2% ; temperature of cross linking reaction 150℃; time of cross linking reaction 4 h. The above-mentioned active material was emulsified by two kinds of self-made polysi-loxane-polyoxyalkylene as main emulsifier and a new silicone emulsion defoamer CX that resisting to high temperature and strong alkali was formed.

关键词

有机硅消泡剂/制备/高温强碱

Key words

silicone defoamer/preparation/high temperature and strong alkali

分类

化学化工

引用本文复制引用

陈晓军,包宗宏,陶刚,周邢..耐高温强碱有机硅消泡剂的研制[J].日用化学工业,2009,39(4):230-233,237,5.

基金项目

国家863计划资助项目(2007AA06A402) (2007AA06A402)

日用化学工业

OA北大核心CSCDCSTPCD

1001-1803

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