波谱学杂志2008,Vol.25Issue(2):281-286,6.
2D NMR对金钱松皮中的一个三萜皂苷进行结构解析
Structure Determination of a Triterpene Saponin Extracted from the Barks of Pseudolarix kaempferi by 2D NMR
摘要
Abstract
A triterpene saponin was extracted from the barks of Pseudorix kaempferi for the first time, and determined to be dammar-24 (25)-ene-3β, 6α, 12β, 20 (S)-tetraol-20-O-β-D-pyranoglucoside on the basis of NMR analysis.The chemical shifts of this compound were completely assigned using 2D NMR spectroscopy.关键词
NMR/全归属/2D NMR/三萜皂苷/dammar-24(25)-ene-3β,6α,12β,20 (S)-tetraol-20-O-β-D- pyranoglucoside/金钱松Key words
NMR, chemical shift, triterpene saponin, pyranoglucoside, Pseudorix kaempferi Gord分类
化学化工引用本文复制引用
岳正刚,肖凯,吴立军,蔺红伟,樊军文,赵杰,李玥,张黎明..2D NMR对金钱松皮中的一个三萜皂苷进行结构解析[J].波谱学杂志,2008,25(2):281-286,6.基金项目
This work was financially supported by grants from the National Scientific Foundation of China (30472141) and Shanghai-SK Development Fund (2004005-t). 国家自然科学基金资助项目(30472141)和上海-SK研究与发展基金(2004005-t)资助. (30472141)