波谱学杂志2008,Vol.25Issue(3):337-341,5.
环维黄杨星D 13C和1H化学位移的全归属
Assignment of 13C and 1H Chemical Shifts of Cyclovirobuxinum D
摘要
Abstract
Cyclovirobuxinum D was isolated from traditional Chinese medicine Buxus icrophylla Sieb. et Zucc, for treating coronary heart disease and arrhythmias. High performance liquid preparation chromatography was used for separation and purification. 13C and 1H chemical shifts of the compound were assigned using 1D and 2D NMR techniques including 1H NMR, 13C NMR, COSY, DEPT, HMQC and HMBC. The structure of the compound was determined from the NMR data.关键词
NMR/归属/2D NMR/环维黄杨星D/黄杨宁生物碱Key words
NMR,chemical shift,2D NMR, cyclovirobuxinum D, Buxus alkaloids分类
化学化工引用本文复制引用
刘洁,李备,杭太俊,陈赞明,张正行..环维黄杨星D 13C和1H化学位移的全归属[J].波谱学杂志,2008,25(3):337-341,5.基金项目
江苏省科学技术厅科技攻关项目(BE2003608).Emphasis item of science-technology bureau Jiangsu province(part of three drug)(BE2003608) (BE2003608)