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电感耦合等离子体发射光谱法测定磷矿石中微量有毒元素铅砷镉

黎香荣 韦万兴 崔翔 罗明贵 陈永欣 马丽方

岩矿测试2009,Vol.28Issue(4):370-372,3.
岩矿测试2009,Vol.28Issue(4):370-372,3.

电感耦合等离子体发射光谱法测定磷矿石中微量有毒元素铅砷镉

Determination of Trace Toxic Elements of Lead, Arsenic and Cadmium in Phosphate Ores by Inductively Coupled Plasma-Atomic Emission Spectrometry

黎香荣 1韦万兴 2崔翔 1罗明贵 1陈永欣 1马丽方1

作者信息

  • 1. 防城港出入境检验检疫局,广西,防城港,538001
  • 2. 广西大学化学化工学院,广西,南宁,530004
  • 折叠

摘要

Abstract

A method for the simultaneous determination of trace elements of lead, arsenic and cadmium in phosphate ores by inductively coupled plasma-atomic emission spectrometry (ICP-AES) was established. The detection limits of the method are 0.042 mg/L for lead, 0.053 mg/L for arsenic and 0.006 mg/L for cadmium. The recoveries of lead, arsenic and cadmium are 109.3%, 94.0% and 90.0% with precision (RSD,n = 11) of 0.86%, 1.36% and 1.08% respectively. The method has been applied to the routine inspection of lead, arsenic and cadmium in phosphate ores with satisfactory results.

关键词

电感耦合等离子体发射光谱法/磷矿石///

Key words

inductively coupled plasma-atomic emission spectrometry/ phosphate ore/ lead/ arsenic/ cadmium

分类

化学化工

引用本文复制引用

黎香荣,韦万兴,崔翔,罗明贵,陈永欣,马丽方..电感耦合等离子体发射光谱法测定磷矿石中微量有毒元素铅砷镉[J].岩矿测试,2009,28(4):370-372,3.

基金项目

广西检验检疫局科研制标项目--磷化工产品中有害元素测定的方法研究项目资助(2008K006) (2008K006)

岩矿测试

OA北大核心CSCDCSTPCD

0254-5357

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