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西瓜、瓜叶及瓜田土壤中乙撑硫脲残留量的液相色谱分析方法研究

纪然 马恒麟 张永刚 刘祖兰

化工环保2001,Vol.21Issue(1):45-49,5.
化工环保2001,Vol.21Issue(1):45-49,5.

西瓜、瓜叶及瓜田土壤中乙撑硫脲残留量的液相色谱分析方法研究

Study on Determination Method of ETU Residue in Watermelon,Watermelon Leaf and Soil by HPLC

纪然 1马恒麟 1张永刚 1刘祖兰1

作者信息

  • 1. 北京化工研究院 环保所,北京 100013
  • 折叠

摘要

Abstract

A determination method of ethylene thiourea (ETU) residue inwatermelon,watermelon leaf and soil by high-performance liquid chromatography (HPIC) has been established.The average recovery efficiency of the method varies from 83.2% to 90.7% and the variation coefficient is less than 12.5% when the samples are spiked at 0.05-10.0 mg/kg.The minimum detectable concentration of ETU in the samples of watermelon,watermelon leaf and soil is 0.02 mg/kg.The method is characterized by low toxicity of the used solvent,higher sensitivity and accuracy.The satisfactory results have been obtained in the application of the method to determine ETU residue in watermelon,watermelon leaf and soil.

关键词

乙撑硫脲/残留分析/高效液相色谱/西瓜/瓜田土壤

分类

资源环境

引用本文复制引用

纪然,马恒麟,张永刚,刘祖兰..西瓜、瓜叶及瓜田土壤中乙撑硫脲残留量的液相色谱分析方法研究[J].化工环保,2001,21(1):45-49,5.

化工环保

OA北大核心CSCD

1006-1878

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