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用薄层色谱法测定骨康片中士的宁和马钱子碱含量

牛晓峰 李维凤 歧林 李延

西安医科大学学报2000,Vol.21Issue(5):478-479,482,3.
西安医科大学学报2000,Vol.21Issue(5):478-479,482,3.

用薄层色谱法测定骨康片中士的宁和马钱子碱含量

Simultaneous determination of strychnine and brucine in Gukang tablet by TLC

牛晓峰 1李维凤 1歧林 1李延1

作者信息

  • 1. 西安交通大学药学院,西安 710061
  • 折叠

摘要

Abstract

Objective To establish the analytical method of strychnine and brucine in Gukang tablet by TLC. Methods Strychnine and brucine in the tablet were separated by TLC using silica stationary phase and toluene/acetone/alcohol/amine solution (4:3:1:2) as developing solution. The detection was at 258nm for strychnine, 301nm brucine. Results The linearities were 0. 9996 and 0. 9999, recoveries were 99.83 % (RSD=1.03%) and 96.09 % (RSD=2.01%), respectively. Conclusion The strychnine and brucine in Gukang tablet were simultaneously detected by TLC. The method can use for controlling quality of the tablet.

关键词

骨康片/士的宁/马钱子碱/双波长薄层扫描法

Key words

Gukang tablet/strychnine/brucine/TLC

分类

医药卫生

引用本文复制引用

牛晓峰,李维凤,歧林,李延..用薄层色谱法测定骨康片中士的宁和马钱子碱含量[J].西安医科大学学报,2000,21(5):478-479,482,3.

西安医科大学学报

OA北大核心CSCDCSTPCD

1671-8259

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