湛江海洋大学学报2005，Vol.25Issue(6)：50-54,5.
不同脱乙酰度壳聚糖接枝丙烯酰胺的合成与表征
Synthesis and Characterization of Graft Acrylamide onto Different Degree of Deacetylation Value of Chitosan
程建华 1胡勇有 1李泗清1
作者信息
- 1. 华南理工大学环境科学与工程学院,广东,广州,510641
- 折叠
摘要
Abstract
Graft copolymer of chitosan was prepared using acrylamide. The grafting reaction was initiated by ammonium persulfate and sodium sulfite. The graft copolymer was characterized by FT-IR,X-ray and SEM techniques. The grafting percentage was also analysed. The grafting percentage showed maxima with 68.5% D.D.(degree of deacetylation) of chitosan under appropriate condition, around 250% grafting percentage was achieved. The best synthesis condition is m(chitosan):m(AM)=1:5; redox indicator 0.3%-0.4% mass fraction of solution; reaction temperature 55-60 ℃; reaction time 2.5-3.0 h.关键词
壳聚糖/水处理/接枝Key words
chitosan/acrylamide/grafting分类
化学化工引用本文复制引用
程建华,胡勇有,李泗清..不同脱乙酰度壳聚糖接枝丙烯酰胺的合成与表征[J].湛江海洋大学学报,2005,25(6):50-54,5.
