国际医药卫生导报2009,Vol.15Issue(8):70-72,3.DOI:10.3760/cma.j.issn.1007-1245.2009.08.030
反相高效液相色谱法测定强筋健骨颗粒中淫羊藿苷的含量
Detecting of Icariin in qiangjinJiangu granulas by RP-HPLC
梁文能 1肖毓芳 1丘振文1
作者信息
- 1. 510405,广州中医药大学第一附属医院
- 折叠
摘要
Abstract
Objective:To detect the contents of lcariin in QiangjinJiangu granulas.Methods The HPLC method was established for the determination of Icariin in Qiangjindiangu granulas.The columu is Kromasi I C18 (4.6mm × 250mm,5μm),mobile phase consisting of acetonitrile-water(25:75).column tempreture 25℃,and the flow rare is 1.0ml/min.The detection wavelength is 270nm.Results A better linear relationship was obtained form 0.01949~0.3898μg of polydatin in plasma,which is with a good correlation coefficient(r=0.9998).The average recovery of ephedrine hydrochloride was,99.90%,RSD was 1.11%.Conelutioa This method is simple and quick.It can be applied to quality control of Qiangjinjiangu granulas.关键词
强筋健骨颗粒/淫羊藿苷/HPLCKey words
lcariin/Qiangjinjiangu granulas/HPLC分类
医药卫生引用本文复制引用
梁文能,肖毓芳,丘振文..反相高效液相色谱法测定强筋健骨颗粒中淫羊藿苷的含量[J].国际医药卫生导报,2009,15(8):70-72,3.