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橡胶树种子油的超临界提取及成分分析

尹桂豪 曹建华 刘春华 李春丽 张世瑞

安徽农业科学2009,Vol.35Issue(19):8814-8815,2.
安徽农业科学2009,Vol.35Issue(19):8814-8815,2.

橡胶树种子油的超临界提取及成分分析

Research on the Supercritical Extraction of Seed Oil from Rubber Tree and Its Composition Analysis

尹桂豪 1曹建华 2刘春华 1李春丽 2张世瑞2

作者信息

  • 1. 中国热带农业科学院橡胶研究所,农业部橡胶树生物学重点开放实验室,海南儋州,571737
  • 2. 中国热带农业科学院分析测试中心,海南海口,571101
  • 折叠

摘要

Abstract

[Objective] The reference for the study on the bio-diesel from rubber tree was provided through the test of supercritical extraction process of seed oil and its composition of fatty acid.[Method] The effect of the extraction temperature, pressure, time and the amount of co-solvent on seed oil was studied with the orthogonal experimental design and the analysis of the composition of fatty acid was conducted.[Results] The best condition of the extraction of rubber seed oil with CO2 supercritical fluid was as follows: the extraction temperature, 45 ℃; the extraction pressure, 40 MPa; the extraction time, 2.5 hours; the amount of ethanol co-solvent, 15% and under these conditions, the extraction rate of rubber tree seed oil was 19.60% and with the color of clear oil.The calculative value of HPLC area normalization was as follows: the myristic acid, 0.13%; the palmitic acid, 9.34%; the palm oil acid, 0.30%; the stearic acid, 8.07%; the oleic acid, 25.90%; the linoleic acid, 39.79%; the linolenic acid, 15.75%; the arachidic acid, 0.34%; the peanut-acid, 0.38% and the unsaturated fatty acid, 82.12% with gas chromatography-mass spectrometry, which was conducive to the preparation of bio-diesel.[Conclusion] The supercritical CO2 fluid extraction of rubber seed oil can be used as the potential preparation of bio-diesel resource.

关键词

超临界CO2萃取/橡胶树种子油/气相色谱-质谱联用

Key words

Supercritical CO2 extraction/Rubber tree seed oil/Gas chromatography-mass spectrometry

分类

农业科技

引用本文复制引用

尹桂豪,曹建华,刘春华,李春丽,张世瑞..橡胶树种子油的超临界提取及成分分析[J].安徽农业科学,2009,35(19):8814-8815,2.

基金项目

中国热带农业科学院橡胶研究所基本科研业务费专项基金项目(XJSYWFZX2008-26). (XJSYWFZX2008-26)

安徽农业科学

OA北大核心CSTPCD

0517-6611

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