煤炭转化2001，Vol.24Issue(1)：93-96,4.
氯铬酸甲胺/硅胶氧化1-萘甲醇制备1-萘甲醛
PREPARATION OF 1-NAPHTHALENE CARBOXYALDEHYDE BY
OXIDIZING 1-NAPHTHYLMETHANOL WITH METHYLAMINE
CHLOROCHROMATE/SILICON DIOXIDE
尹学琼 1魏贤勇 1宗志敏 2林强3
作者信息
- 1. 大连理工大学
- 2. 中国矿业大学化工学院,
- 3. 海南大学理工学院,
- 折叠
摘要
Abstract
This paper discussed a new method for synthesizing 1-naphthalene carboxyaldehyde (1-NA) by oxidizing 1-naphthylmethanol with methylamine chlorochromate supported by silicon dioxide. Through investigating the effects of temperature, concentration of 1-naphthylmethanol, amount of oxidant, and solvents, it was found that 1-NA can be selectively obtained at room temperature. The selectivity reached 90.2%.关键词
MCC/硅胶,1-萘甲醇,1-萘甲醛,氧化分类
化学化工引用本文复制引用
尹学琼,魏贤勇,宗志敏,林强..氯铬酸甲胺/硅胶氧化1-萘甲醇制备1-萘甲醛[J].煤炭转化,2001,24(1):93-96,4.
