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磁性核壳Fe3O4/Ag纳米复合粒子的制备及性能

章桥新 杨丽宁 张佳明 官建国 王一龙

硅酸盐学报2007,Vol.35Issue(8):987-990,4.
硅酸盐学报2007,Vol.35Issue(8):987-990,4.

磁性核壳Fe3O4/Ag纳米复合粒子的制备及性能

PREPARATION OF MAGNETIC CORE-SHELL Fe3O4/Ag NANOPARTICLES AND ITS PROPERTIES

章桥新 1杨丽宁 2张佳明 2官建国 2王一龙2

作者信息

  • 1. 武汉理工大学机电工程学院武汉理工大学,材料复合新技术国家重点实验室,武汉,430070
  • 2. 武汉理工大学,材料复合新技术国家重点实验室,武汉,430070
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摘要

Abstract

Fe3O4/Ag core-shell nanoparticles were prepared by the reduction of Ag[(NH3)2]+ with formaldehyde as reductant, and mercapto-propyl-trimethoxy-silane as an additive. The nanocomposite particles were characterized by X-ray diffraction, field-emission-scanning electron microscopy, differential thermal analysis, vibrating sample magnetometry and HL-5 hall effect testing. The results show that the size distributions of the core-shell Fe3O4/Ag nanocomposites averaged 40-60 nm, with a thickness of 10-15 nm of Ag layer.The volume resistivity of the nanocomposites is 7.757 3×10-4 Ω·cm and the saturation magnetization is 26.37 A·m2/kg.

关键词

磁性核壳/四氧化三铁/银/纳米复合粒子/电磁性能

Key words

magnetic core-shell/ferroferric oxide/silver/nanocomposite/electromagnetic properties

分类

化学化工

引用本文复制引用

章桥新,杨丽宁,张佳明,官建国,王一龙..磁性核壳Fe3O4/Ag纳米复合粒子的制备及性能[J].硅酸盐学报,2007,35(8):987-990,4.

基金项目

国家"863"计划(2006AA03Z461)和国防预研基金计划(51447020105QT6903)资助项目. (2006AA03Z461)

硅酸盐学报

OA北大核心CSCDCSTPCD

0454-5648

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