人工晶体学报2011，Vol.40Issue(1)：139-143,5.
模板剂对微波水热合成CdS微晶相组成、形貌及光学性能的影响
Influence of Templates on the Phase Composition, Morphology and Optical Performance of CdS Microcrystalline Prepared by Microwave Hydrothermal Process
摘要
Abstract
Cadmium sulphide (CdS) microcrystallites with different morphology had been prepared by microwave hydrothermal(M-H) process using cadmium chloride and sodium thiosulfate as raw materials and citric acid, ethylene diamine tetraacetic acid (EDTA), hexamethylenetetramine and polyvinylpyrrolidone (PVP) as template.The products were characterized by X-ray diffraction(XRD),scanning electron microscopy ( SEM ), EDS and transmission electron microscopy (TEM).The optical properties of the prepared CdS microcrystallites with varied shape were characterized by ultraviolet-vis.The results show that the spherical, flower-like and rod-like CdS crystals could be prepared using different templates, and the as-prepared products are well crystallized.Obvious blue-shift are observed in the UV-Vis absorption of CdS products.关键词
CdS微晶/微波水热/模板剂/形貌Key words
CdS microcrystalline/ microwave hydrothermal process/ template/ morphology分类
化学化工引用本文复制引用
胡宝云,黄剑锋,张钦峰,张海,曹丽云,吴建鹏..模板剂对微波水热合成CdS微晶相组成、形貌及光学性能的影响[J].人工晶体学报,2011,40(1):139-143,5.基金项目
国家自然科学基金(50942047)资助项目 （50942047）
教育部新世纪优秀人才支持计划基金(NECT-06-0893) （NECT-06-0893）
教育部博士点基金 (20070708001) （20070708001）
陕西省自然科学基金(2010JM6001)资助项目 （2010JM6001）
陕西科技大学科研创新团队基金(TD09-05) （TD09-05）
陕西科技大学博士科研基金(BS08-09) （BS08-09）
陕西科技大学研究生创新基金 （）
