河南农业科学2011,Vol.40Issue(1):90-93,4.
2,5-二苯乙炔噻吩β-环糊精微胶囊的研制与性能研究
Preparation and Properties of the Inclusion Compound of 2,5-Diphenylethyny1thiophene with β-Cyclodextrin
摘要
Abstract
The 2,5-diphenylethynylthiophene(DPET) with β-cyclodextrin was prepared in inclusion compound. The ratio of DPET to cyclodetrin, the temperature and the time of reaction as the dominating factors were optimized by orthogonal experiment. The results showed that the yield of DPET inclusion compound with β-cyclodextrin was more than 60% when the mass ratio of DPET to cyclodextirn was 1: 40 and the reaction was under 40-60℃ for 0. 5-2 hours. The half life of DPET was 11:08 min under ultraviolet while it extended to 4.63 h for DPET β-cyclodextrin inclusion compound. The bioactivity of the compound was evaluated with the third-instar larvae of Plutella xylostella L. Pretreated with ultraviolet, DPET β-cyclodextrin inclusion compound showed higher activity than DPET, which indicated that the inclusion compound with β-cyclodextrin could retard the DPETs decompositon under light.关键词
2,5-二苯乙炔噻吩/β-环糊精/微胶囊/光活化农药Key words
2,5-Diphenylethynylthiophene/ β-cyclodextrin/ Inclusion compound / Light-activated insecticide分类
农业科技引用本文复制引用
吴仁海,王恒亮,张永超,孙建伟,杨东亚..2,5-二苯乙炔噻吩β-环糊精微胶囊的研制与性能研究[J].河南农业科学,2011,40(1):90-93,4.基金项目
郑州市金水区技术研究与开发经费支持项目(金科字[2008]18号) (金科字[2008]18号)
河南省农科院植保所青年基金项目 ()