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高温固相合成NixZn1-xFe2O4铁氧体及物相组成分析

刘树信

中国粉体技术2011,Vol.17Issue(1):29-31,3.
中国粉体技术2011,Vol.17Issue(1):29-31,3.DOI:10.3969/j.issn.1008-5548.2011.01.008

高温固相合成NixZn1-xFe2O4铁氧体及物相组成分析

Synthesis and Phase Analysis of NixZn1-xFe2O4 by High Temperature Solid State Reaction

刘树信1

作者信息

  • 1. 绵阳师范学院,化学与化学工程学院,绵阳,四川,621010
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摘要

Abstract

NixZn1-xFe2O4 ( x =0~0.9) ferrites were synthesized by high temperature solid state reaction with Fe2O3, ZnO and NiO as raw materials.The mixturer of the raw materials and the sample were analyzed by TGSDTA and XRD. The results showed that all the products were single phase of spinel structure ferrites belonged to cubic crystal system and all the crystals were crystallized with good integrality. No single phase of NiO, ZrO and Fe2O3 existed in the products. X-ray diffraction peaks of samples gradually shifted to big angle and the crystal cell parameters reduced gradually with the increasing of the content of Ni. These phenomenons were brought about by the size of the metal ions and the relative contents ofZn2+, Fe3+ and Ni2+.

关键词

镍-锌铁氧体/物相组成/高温固相反应

分类

通用工业技术

引用本文复制引用

刘树信..高温固相合成NixZn1-xFe2O4铁氧体及物相组成分析[J].中国粉体技术,2011,17(1):29-31,3.

基金项目

四川省科技厅科研项目,编号:2006J13-034 ()

四川省教育厅科研项目,编号:2006A139. ()

中国粉体技术

OA北大核心CSTPCD

1008-5548

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