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碳黑比表面积标准物质的研制

王海 冯颖 宋小平

中国粉体技术2011,Vol.17Issue(1):72-75,4.
中国粉体技术2011,Vol.17Issue(1):72-75,4.DOI:10.3969/j.issn.1008-5548.2011.01.020

碳黑比表面积标准物质的研制

Development of Certified Reference Materials for Specific Surface Area of Carbon Black

王海 1冯颖 2宋小平1

作者信息

  • 1. 中国计量科学研究院,北京,100013
  • 2. 北京联合大学,生物化学工程学院,北京,100023
  • 折叠

摘要

Abstract

The three commercial carbon blacks were used as the candidates for certified reference materials (CRMs) of specific surface area and subpackaged in the transparent glass bottles sealed with screw cap by means of cross riffling method. The homogeneity and stability tests showed that the carbon black CRMs were homogeneous and stable for at least 18 months,respectively. The BET specific surface areas of 104.6, 29.9, 8.96 m2/g were certified by internationally recognized nitrogen physical adsorption method among eight validated separate laboratories. Compared with the similar CRMs in the world, it was showed that the uncertainties (2.1%, 2.3% and 3.2%) of three carbon black CRMs came up to advanced world level.

关键词

标准物质/比表面积/碳黑

分类

通用工业技术

引用本文复制引用

王海,冯颖,宋小平..碳黑比表面积标准物质的研制[J].中国粉体技术,2011,17(1):72-75,4.

基金项目

国家科技基础条件平台建设项目,编号:2005DKA10800,2005DKA10806. ()

中国粉体技术

OA北大核心CSTPCD

1008-5548

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