中国组织工程研究与临床康复2011，Vol.15Issue(3)：441-444,4.DOI:10.3969/j.issn.1673-8225.2011.03.015
一种碳/碳复合材料表面制备高结合强度羟基磷灰石涂层的新方法
A novel method for preparing adherent hydroxyapatite coating on carbon/carbon composite surface
摘要
Abstract
BACKGROUND:At present, there are many methods for preparing hydroxyapatite (HA) coating on carbon/carbon composite surface, but the bonding strength between the prepared coating and the substrate is not high.OBJECTIVE:To propose a novel method for preparing HA coating with high bonding strength on carbon/carbon composite surface.METHODS:Firstly, monetite coating was deposited on carbon/carbon composite using induction heating technique, and then the monetite coating was converted to HA by hydrothermal method in ammonia solution. The morphology of the coating was observed under scanning electron microscopy, the critical load of HA coating was determined using scratch test, and shear strength was detected with extrusion method.RESULTS AND CONCLUSION:Using induction heat deposition method, dense block anhydrous dicalcium phosphate coating with grain structure was prepared in the carbon/carbon composite surface, and then transformed into dense HA coating with good crystals by hydrothermal method. The critical load of HA coating is 13.31 N and shear strength is 47 MPa.关键词
碳/碳复合材料/羟基磷灰石/高频感应加热沉积/水热反应/涂层分类
医药卫生引用本文复制引用
李冬梅,熊信柏,邹春莉,马楚凡..一种碳/碳复合材料表面制备高结合强度羟基磷灰石涂层的新方法[J].中国组织工程研究与临床康复,2011,15(3):441-444,4.基金项目
陕西省科技计划项目(2008K14-03),国家自然科学基金资助(50702034),深圳市科技计划项目(PT200805200295A). （2008K14-03）
