中医药导报2011,Vol.17Issue(1):83-85,3.
HPLC法测定精制冠心片中丹酚酸B的含量
Content Determination 0f Salvianolic Acid B in Jingzhi Guanxin Tablet by HPLC
蒋珍藕 1兰宝强 1邱宏聪 1李茂1
作者信息
- 1. 广西中医药研究院,广西,南宁,530022
- 折叠
摘要
Abstract
Objective:To establish the content determination method of salvianolic acid B in Jingzhi Guanxin Tablet by HPLC. Methods:C18 colum was adpoted at the column temperature 25℃ ,the mobile phase consisted of acetonitrile-methanol-methanoic acid-water (10∶30∶0.5∶59.5)with flow rate 1.0 mL/min and the detection wavelength was 286 nm.Results :The content of salvianolic acid B was determined by HPLC, The results showed good linear relationship, the average recovery rate was 98.51% and RSD value was 1.72%(n=6). Conclusion:The established method is convenient and feasible and accurate and reliable and can be used for the quality control of Jingzhi Guanxin Tablet.关键词
精制冠心片/丹酚酸B/HPLC/含量测定分类
医药卫生引用本文复制引用
蒋珍藕,兰宝强,邱宏聪,李茂..HPLC法测定精制冠心片中丹酚酸B的含量[J].中医药导报,2011,17(1):83-85,3.