分析化学2011，Vol.39Issue(1)：107-110,4.
基于两维扫描高场不对称离子迁移谱技术检测挥发酚
Volatile Phenolic Compounds Detection by 2D Scanning High-Field Asymmetric Waveform Ion Mobility Spectrometry
摘要
Abstract
Detection of phenol, 2-methylphenol, 3-methylphenol, 4-methylphenol and 2,4-dichlorophenol was carried out by laboratory-built high-field asymmetric waveform ion mobility spectrometer (FAIMS). Separation of those compounds was enhanced by sweeping compensation voltage(CV)under different dispersion voltage(DV) values. Best separation result of 2-methylphenol and 4-methylphenol was obtained at high-field strength of 1.6 × 104 V/cm, optimum separation of remaining compounds was obtained at high-field strength larger than 1.8 × 104 V/cm. high-field mobility of those compounds was reported for the first time. Experiment results showed that the sensitivity was decreased and the resolution was usually increased by increasing high-field strength. When the highfield strength was set at 2.0×104 V/cm, the limit of detection for 2-methylphenol was 1 μg/L.关键词
高场不对称离子迁移谱/挥发酚Key words
High-field asymmetric waveform ion mobility spectrometry/ Volatile phenolic compounds引用本文复制引用
李庄,林丙涛,陈池来,刘英,孔德义,程玉鹏,王电令,王焕钦..基于两维扫描高场不对称离子迁移谱技术检测挥发酚[J].分析化学,2011,39(1):107-110,4.基金项目
本文系国家自然科学基金(No.60871037)和863计划(No.2007AA04Z341)资助项目 （No.60871037）
