广东药学院学报2011，Vol.27Issue(1)：27-30,4.DOI:10.3969/j.issn.1006-8783.2011.01.007
β-烯胺酮类化合物的合成与结构鉴定
Synthesis and identification of β-Enamino ketones
摘要
Abstract
Objective To establish a new route for the synthesis of β-Enamino ketone. Methods 9 β-Enamino ketones were synthesized at room temperature, using α-methyl ketones as starting materials. via two steps reaction of formylation and ketone-amine condensation. Results The structures of title compounds were confirmed by IR, MS, and 1H-NMR and XRD analysis. Conclusion The improved procedure has the advantage of low costing of starting material. and the convenient simple route, which is suitable for large scale of production.关键词
β-烯胺酮/碳负离子/甲酰化分类
医药卫生引用本文复制引用
刘丰收,申东升,邓爵安,谭诚..β-烯胺酮类化合物的合成与结构鉴定[J].广东药学院学报,2011,27(1):27-30,4.基金项目
广州市番禺区科技攻关项目资助(2010-z-13-1) （2010-z-13-1）
