硅酸盐通报2011，Vol.30Issue(1)：83-88,6.
TiO2溶胶稳定化制备工艺及机理研究
Study on the Preparation Technology and Mechanism of the Stabilization of TiO2 Sol
摘要
Abstract
A kind of TiO2 sol, which had good stability at room temperature, was prepared by sol-gel process, using tetrabutyl titanate (TBOT) as precursor, ethanol as solvent, hydrochloric acid as catalyst.The effects of reaction temperature, amounts of solvent, catalyst and water on the stability of sol were studied. And the degree of influence of all factors on the stability of sol was analysed by L9 (34)orthogonal test. The result showed the optimum technological parameters are as follow: reaction temperature 30℃, the mole ratio of TBOT to ethanol, hydrochloric acid, water 1/32, 2, 1,respectively. At last, the specific mechanism of sol-gel process was preliminarily studied from the point of view of acid catalysis.关键词
稳定化/溶胶-凝胶/TiO2溶胶/胶凝时间/正交试验Key words
stabilization/ sol-gel/ TiO2 sol/ gelation time/ orthogonal test分类
通用工业技术引用本文复制引用
向洪平,沈汝梁,邓浩强,戴如勇,吕俊佳,葛建芳..TiO2溶胶稳定化制备工艺及机理研究[J].硅酸盐通报,2011,30(1):83-88,6.基金项目
仲恺农业工程学院校级科研基金项目(G3100098) （G3100098）
校级研究生创新基金项目(H1410009) （H1410009）
