华中师范大学学报（自然科学版）2011，Vol.45Issue(1)：63-67,5.
"一锅法"合成(芳氨基甲基)苯酚
One-pot synthesis of arylaminomethyl phenols
摘要
Abstract
A series of arylaminomethyl phenols were prepared by "one-pot" process and fractional step methods using salicylaldehyde or 4-hydroxybenzaldehyde and substituted anilines as starting materials. The products were obtained in higher yields with "one-pot" synthesis method. For both methods, the yields had closed relationship with the substituents on the phenyl group connected with the nitrogen atom.. OCH3 ＞ CH3 ＞ H ＞ Cl. But, the "one-pot"process was much simpler, cost less solvent and produced less waste than the fractional step method, and is very efficient and practicable for the synthesis of substituted aminomethylphenols. The structures of the products were characterized by IR,1H NMR,13C NMR.关键词
芳氨基甲基苯酚/合成/一锅法Key words
arylaminomethyl phenol/ synthesis/ "one-pot" process分类
化学化工引用本文复制引用
唐子龙,常书红,张超逸,颜林,刘汉文.."一锅法"合成(芳氨基甲基)苯酚[J].华中师范大学学报（自然科学版）,2011,45(1):63-67,5.基金项目
国家自然科学基金项目(21042011) （21042011）
湖南省教育厅重点科研项目(10A034) （10A034）
中国博士后科学基金项目(20100471228) （20100471228）
湖南省博士后科学基金项目(2010RS4033). （2010RS4033）
