波谱学杂志2011,Vol.28Issue(1):142-152,11.
岗梅根中一个三萜类化合物的NMR信号表征
Characterization of NMR Signals of a Tirterpenoid Isolated from Radix of Ilex asprella
摘要
Abstract
The chemical constituents of the radix of Ilex asprella, separated by column chromatography, were analyzed by MS, 1H NMR, 13C NMR, DEPT, 1H-1H COSY, HSQC and HMBC. A triterpenoid, Urs-12-ene-3β, 28-diol, 3-acetate, was isolated from the chloroform extract of the radix of Ilex asprella. The 1H and 13C NMR chemical shifts of the compound were assigned.关键词
核磁共振(NMR)/归属/三萜类化合物/岗梅根Key words
NMR/ chemical shift assignment/ tirterpenoid/ radix of Ilex asprella分类
数理科学引用本文复制引用
黄锦茶,陈丰连,曾元儿,曹骋,徐鸿华..岗梅根中一个三萜类化合物的NMR信号表征[J].波谱学杂志,2011,28(1):142-152,11.基金项目
广东省科技计划资助项目(2008A030101009,2010B06900073,2010B031900007) (2008A030101009,2010B06900073,2010B031900007)
广东省重大科技资助专项(2007A032200001). (2007A032200001)