天津工业大学学报2011，Vol.30Issue(2)：69-72,4.
线性体合成反应性氨基硅油的工艺研究
Study on synthyesis of reactive aminosilicone from linear polydimethylsiloxane
张志立 1郑帼1
作者信息
- 1. 天津工业大学纺织纤维界面处理技术工程中心,天津300160
- 折叠
摘要
Abstract
Reactive aminosilicone is synthesized by hydrolysis and condensation between linear polydimethylsiloxane and N -β-aminoethyl-γ-aminopropylmethydimethoxysilane using sodium hydroxide as catalyst.The effects of catalyst dosage, the amount of aminosilane coupling agent, the reaction temperature and time on the amine value and viscosity of aminosilicone are investigated.The product is characterized by means of FT- IR and 1H NMR.The results show that the amine value of reative aminosilicone raises with coupling agent dosage increasing; its viscosity increases with coupling agent dosage descending, reaction temperature heighten and time extending,and viscosity changes wavily with catalyst dosage increasing.关键词
线性体/反应性氨基硅油/氨值/织物柔软剂Key words
linear polydimethylsiloxane/ reactive aminosilicone/ amine value/ fabric softener分类
轻工纺织引用本文复制引用
张志立,郑帼..线性体合成反应性氨基硅油的工艺研究[J].天津工业大学学报,2011,30(2):69-72,4.
