福州大学学报（自然科学版）2011，Vol.39Issue(2)：302-306,5.DOI:CNKI:35-1117/N.20110402.1009.024
二茂铁甲酰基硫脲类异构体衍生物的高效液相色谱研究
Study on high performance liquid chromatography of ferrocene- containing acetylthiourea isomeric derivatives
摘要
Abstract
The binary mobile phase optimum composition as the three comers of the solvent triangle is calculated with the theory established by Schoemaker, which is gradient elution for rapid selection of isocratic conditions. The binary mobile phases are methanol- water, THF -water and acetonitrile water. Then, the optimization of the quaternary mobile phase composition is achieved by using the o verlapping resolution method, and finally the optimized results are used to separate the six N - ferro cenoyl - N' - arylthiourea isomeric derivatives.关键词
高效液相色谱/重叠分辨率法/最佳化/二茂铁衍生物Key words
high performance liquid chromatography/ overlapping resolution/ optimization/ ferrocenyl derivatives分类
化学化工引用本文复制引用
张国兰,傅谢学,谢莉莉,王文峰,袁耀锋..二茂铁甲酰基硫脲类异构体衍生物的高效液相色谱研究[J].福州大学学报（自然科学版）,2011,39(2):302-306,5.基金项目
福建省自然科学基金资助项目(2009J05028) （2009J05028）
福建省科技重点资助项目(2009H0021) （2009H0021）
福建省教育厅科研资助项目(JA07017) （JA07017）
