农业工程学报2011,Vol.27Issue(4):174-178,5.DOI:10.3969/j.issn.1002-6819.2011.04.030
柴油机多环芳香烃类污染物的测量方法
Measurement method of polycyclic aromatic hydrocarbon emission of diesel engine
摘要
Abstract
The polycyclic aromatic hydrocarbons (PAHs) of diesel engine exhaust were measured by a method of using Teflon filter and XAD-2 collection, as well as ultrasonic extraction, Soxhlet extraction and GC-MS analysis.The results showed that concentration of different component in PAHs and the peak area had a good linear relationship in the experimental concentration range, and the linear correlation coefficient was above 0.99.Linear range was wider with 0.0125-80μg/mL.The method was more efficient for samples collection, and extraction efficiency was above 95%.The method had more repeatability, and relative standard deviation was less than 15%.Recoveries of filter samples were 70.1%-95.9%, the recoveries of adsorbent samples were 77.0%-102.6%.The method had higher sensitivity with minimum detection limit of 0.04 μg/m3, so it can be used for rapid analysis of PAHs content on diesel engine.关键词
多环芳香烃/柴油机/排放/气质联用分析Key words
polycyclic aromatic hydrocarbons/ diesel engine/ emission/ GC/MS analysis分类
能源科技引用本文复制引用
王忠,安玉光,许广举,王宇成,王小哲..柴油机多环芳香烃类污染物的测量方法[J].农业工程学报,2011,27(4):174-178,5.基金项目
国家自然科学基金项目(50776042) (50776042)
江苏省高校自然科学重大基础研究项目(10KJA470009) (10KJA470009)
江苏省博士创新基金(CX10B_261Z) (CX10B_261Z)
江苏江苏高校优势学科建设工程资助项目. ()