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气相色谱质谱联用结合保留指数分析薄荷挥发性成分

张玉朋 张莹 容蓉 吕青涛 李峰

山东中医药大学学报2011,Vol.35Issue(3):247-249,3.
山东中医药大学学报2011,Vol.35Issue(3):247-249,3.

气相色谱质谱联用结合保留指数分析薄荷挥发性成分

Volatile compounds in herba menthae analyzed by GC-MS combined with Kovats rention indices

张玉朋 1张莹 1容蓉 1吕青涛 1李峰1

作者信息

  • 1. 山东中医药大学药学院,山东,济南,250355
  • 折叠

摘要

Abstract

Objective:To analyze the volatile compounds in herba menthae(HM). Methods :Using steam distillation,volatile components in HM were analyzed and identified by gas chromatography-mass spectroscopy(GC-MS) combined with Kovats retention indices(KI). Results:Total 70 components in HM were detected by GC-MS and 36 main volatile compounds were identified by MS combined with KI. Compounds with high contents were as follows:trans-5-methyl-2-( 1 -methylethyl ) -cyclohexanone (26.08%), pulegone ( 11.58% ), β-cadinene (6.11% ) and caryophyllene (8.04%). Conclusion:Using MS combined with KI is a accurate way for the identification of volatile compounds in HM.

关键词

薄荷/挥发性成分/GC-MS/保留指数

Key words

herba menthae /volatile compounds/ GC-MS/ Kovats retention indices

分类

医药卫生

引用本文复制引用

张玉朋,张莹,容蓉,吕青涛,李峰..气相色谱质谱联用结合保留指数分析薄荷挥发性成分[J].山东中医药大学学报,2011,35(3):247-249,3.

基金项目

国家重点基础研究发展计划(973计划)资助项目(编号:2007CB512601) (973计划)

山东中医药大学学报

OACSTPCD

1007-659X

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