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砷钼杂多酸分光光度法测定三七中总砷含量

陈瑞 刘卫 黄兆龙 易中周 闵勇

安徽农业科学2011,Vol.39Issue(8):4534-4535,2.
安徽农业科学2011,Vol.39Issue(8):4534-4535,2.

砷钼杂多酸分光光度法测定三七中总砷含量

Determination of As in Panax notoginseng( Burk. ) F.H. Chen by Heteromolybdoarsenic Acid Spectrophotometry

陈瑞 1刘卫 1黄兆龙 2易中周 1闵勇2

作者信息

  • 1. 红河学院理学院,云南蒙自,661100
  • 2. 云南省天然药物与化学生物学重点实验室,云南蒙自,661100
  • 折叠

摘要

Abstract

[ Objective ] To obtain a rap( )termination method for arsenic from Panax notoginseng ( Burk. ) F. H. Chen. [ Method ] Content of As was determined by heteromolybdoarsenic acid spectrophotometry, and the developing conditions were optimized. [ Result] The optimum developing conditions were :color developing agent amount of 5.0 mi,color developing temperature of 40 ℃ and developing duration of 30 min.When the concentration of standard As Ⅲ solution ranged from 0 to 0.04 μg/ml, the linear relationship between concentration and absorbance was good (r =0.996 6). Arsenic was not detected in sample. [ Result ] High in precision and good in stability,the method can be used as the determination method for As from Panax notoginseng ( Burk. ) F. H. Chen.

关键词

砷钼杂多酸分光光度法/三七/总砷

Key words

Heteromolybdoarsenic acid spectrophotometry/ Panax notoginseng (Burk.)F. H. Chen/ Arsenic

分类

农业科技

引用本文复制引用

陈瑞,刘卫,黄兆龙,易中周,闵勇..砷钼杂多酸分光光度法测定三七中总砷含量[J].安徽农业科学,2011,39(8):4534-4535,2.

基金项目

国家公益性项目(200810998). (200810998)

安徽农业科学

0517-6611

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