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反相高效液相色谱法测定羚贝止咳糖浆中橙皮苷含量

胡安青

中国药业2011,Vol.20Issue(14):39-40,2.
中国药业2011,Vol.20Issue(14):39-40,2.

反相高效液相色谱法测定羚贝止咳糖浆中橙皮苷含量

Determination of Hesperidin in Lingbei Cough Syrup by RP-HPLC

胡安青1

作者信息

  • 1. 江苏省镇江药品检验所,江苏镇江212003
  • 折叠

摘要

Abstract

Objective To determine the content of hesperidin in Lingbei Cough Syrup by RP - HPLC. Methods The determination was carried out on the Symmetry C18 column. The mobile phase was consisted of CH3OH -CH3COOH - H2O(35 ∶ 4 ∶ 61). The flow rate was 1.0 mL/min and the detective wavelength was at 283 nm. Results The content of hesperidin could be determined by RP - HPLC. The linear conrentration range of hesperidin was 84. 0 - 840. 0 μg/mL. The average recovery rate was 101. 75% , RSD was 0. 32% ( n =6). Conclusion The method is simple and accurate,which can be used to control the quality of Lingbei Cough Syrup.

关键词

血府逐瘀口服液/橙皮苷/反相高效液相色谱法

Key words

lingbei cough syrup/ hesperidin/ RP - HPLC

分类

医药卫生

引用本文复制引用

胡安青..反相高效液相色谱法测定羚贝止咳糖浆中橙皮苷含量[J].中国药业,2011,20(14):39-40,2.

中国药业

OACSTPCD

1006-4931

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