中国药业2011,Vol.20Issue(14):39-40,2.
反相高效液相色谱法测定羚贝止咳糖浆中橙皮苷含量
Determination of Hesperidin in Lingbei Cough Syrup by RP-HPLC
胡安青1
作者信息
- 1. 江苏省镇江药品检验所,江苏镇江212003
- 折叠
摘要
Abstract
Objective To determine the content of hesperidin in Lingbei Cough Syrup by RP - HPLC. Methods The determination was carried out on the Symmetry C18 column. The mobile phase was consisted of CH3OH -CH3COOH - H2O(35 ∶ 4 ∶ 61). The flow rate was 1.0 mL/min and the detective wavelength was at 283 nm. Results The content of hesperidin could be determined by RP - HPLC. The linear conrentration range of hesperidin was 84. 0 - 840. 0 μg/mL. The average recovery rate was 101. 75% , RSD was 0. 32% ( n =6). Conclusion The method is simple and accurate,which can be used to control the quality of Lingbei Cough Syrup.关键词
血府逐瘀口服液/橙皮苷/反相高效液相色谱法Key words
lingbei cough syrup/ hesperidin/ RP - HPLC分类
医药卫生引用本文复制引用
胡安青..反相高效液相色谱法测定羚贝止咳糖浆中橙皮苷含量[J].中国药业,2011,20(14):39-40,2.