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差示扫描量热分析测定外掺氧化镁水泥浆体中的氢氧化镁

陈福松 徐玲玲

硅酸盐通报2011,Vol.30Issue(2):256-260,5.
硅酸盐通报2011,Vol.30Issue(2):256-260,5.

差示扫描量热分析测定外掺氧化镁水泥浆体中的氢氧化镁

Determination of Magnesium Hydroxide in Cement Paste Added with Magnesia by Differential Scanning Calorimetry

陈福松 1徐玲玲2

作者信息

  • 1. 南京工业大学材料科学与工程学院,南京,210009
  • 2. 江苏名和建设有限公司,镇江,212000
  • 折叠

摘要

Abstract

This paper introduces the differential scanning calorimetry(DSC) incremental method which is used to determine magnesium hydroxide in cement paste added with magnesia and on this basis, proposes the once-incement method used to determine magnesium hydroxide also. Besides the paper evaluates the accuracy of these two methods by recovery rate. The result shows that the recovery rate of magnesium hydroxide in cement paste added with magnesia is more than 98.5% by DSC incremental method and more than 97.5% by once-incement method. Though the DSC incremental method has high accuracy in determination of magnesium hydroxide in cement paste added with magnesia and the once-incement method is slightly lower in accuracy, the once-incement method is superior to the DSC incremental method in simplified operation and can be used to determine magnesium hydroxide also.

关键词

差示扫描量热分析/增量法/Mg(OH)2/水泥

Key words

differential scanning calorimetry/ incremental method/ magnesium hydroxide/ cement

分类

建筑与水利

引用本文复制引用

陈福松,徐玲玲..差示扫描量热分析测定外掺氧化镁水泥浆体中的氢氧化镁[J].硅酸盐通报,2011,30(2):256-260,5.

硅酸盐通报

OA北大核心CSCDCSTPCD

1001-1625

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