新型介孔材料的热及水热稳定性OA北大核心CSCDCSTPCD
Thermal and Hydrothermal Stabilities of Novel Mesoporous Material
以柠檬酸为成孔剂,正硅酸乙酯为硅源,硫酸铝为铝源,在水热条件下合成一种新型介孔硅铝材料,并采用X射线衍射(XRD)和透射电镜(TEM)对样品进行表征.N2吸附-脱附结果表明,新型介孔材料在1 173 K的高温条件下焙烧5 h以及在沸水中分别处理48,96,192,288 h后,样品依然保持较好的介孔结构,表明样品具有较好的热及水热稳定性.
A novel mesoporous aluminosilicate material was synthesized with citric acid as pore forming agent,tetraethoxysilane (TEOS) and Al2(SO4).3 · 18H2O as silica source and aluminum source, respectively. The sample was characterized by XRD and TEM. The results of N2 adsorption-desorption showed that the mesoporous structure of novel material was maintained under the condition of both calcinations at 1 173 K in air for 5 h and treatment in the boiling water for 48…查看全部>>
徐玲;关利国;阚秋斌
内蒙古民族大学,化学化工学院,内蒙古,通辽,028043内蒙古民族大学,化学化工学院,内蒙古,通辽,028043吉林大学,化学学院,长春,130021
化学化工
介孔材料热稳定性水热稳定性
mesoporous material thermal stability hydrothermal stability
《吉林大学学报（理学版）》 2011 (2)
323-326,4
内蒙古自治区高等学校科研项目(批准号:NJZY08084)和内蒙古民族大学博士科研启动基金(批准号:BS190).
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