中国药业2011,Vol.20Issue(8):34-35,2.
高效液相色谱法测定小儿早熟抗胶囊中栀子苷含量
Determination of Geniposide in Xiao'er Zaoshukang Capsule by HPLC
摘要
Abstract
Objective To develop a HPLC method for the determination of geniposide in Xiso'er Zaoshoukang Capsule. Methods The Eclipse-C18 column(250 mm ×4.6 mm, 5 μm) was used with the mobile phase of acetonitrile-water(12: 88), the flow rate of 1.0 mL/min and the detection wavelength of 238 nm. Results The good linear relationship for geniposide was in the ranges of 3.625-580.0 μg/mL( r = 1. 000 0, n =7). The average recovery rate was 97.91%, RSD = 1.33% ( n =9). Conclusion This HPLC method is simple, quick,rapids and accurate, which can be used for the quality control of xiao'er zaoshukang capsule.关键词
小儿早熟抗胶囊/栀子苷/高效液相色谱法/含量测定分类
医药卫生引用本文复制引用
郑国平,李彬..高效液相色谱法测定小儿早熟抗胶囊中栀子苷含量[J].中国药业,2011,20(8):34-35,2.基金项目
浙江省中医药科技计划项目,项目编号:2008JA010. ()