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高效液相色谱法测定气阴养骨片中马钱苷含量

吴俊贤 陈楷斌 赵琦君 陈志平

中国药业2011,Vol.20Issue(9):24-25,2.
中国药业2011,Vol.20Issue(9):24-25,2.

高效液相色谱法测定气阴养骨片中马钱苷含量

Determination of Loganin in Qiyinyanggu Tablets by HPLC

吴俊贤 1陈楷斌 2赵琦君 3陈志平4

作者信息

  • 1. 广东省河源市药品检验所,广东,河源,517000
  • 2. 广东医学院,广东,东莞,523808
  • 3. 广州中医药大学,广东,广州,510006
  • 4. 广东省河源市中医院,广东,河源,517000
  • 折叠

摘要

Abstract

Objective To establish an HPLC method for determination of loganin in Qiyinyanggu Tablets. Methods The method was established by using Gemini C18 110R column (250 mm ×4. 60 mm, 5 μm),the mobile phase was acetonitrile-water(15∶85), the detection wavelength was 236 nm, column temperature was 40 ℃. Results The linear range of loganin was 0. 048-0. 24 μg; the average recovery rate was 100. 00%, RSD was 0( n = 6). Conclusion This method can accurately determine the content of loganin.

关键词

高效液相色语法/气阴养骨片/马钱苷/含量测定

分类

医药卫生

引用本文复制引用

吴俊贤,陈楷斌,赵琦君,陈志平..高效液相色谱法测定气阴养骨片中马钱苷含量[J].中国药业,2011,20(9):24-25,2.

中国药业

OACSTPCD

1006-4931

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