四川师范大学学报（自然科学版）2011，Vol.34Issue(3)：388-391,4.DOI:10.3969/j.issn.1001-8395.2011.03.023
不活泼芳胺异硫氰酸酯的合成研究
The Study on Synthesis Inactive Aromatic Amine Isothiocyanates
摘要
Abstract
Inactive aromatic amine isothiocyanates were synthesized with the inactive arylamines, carbon disulfide, 1,4-diazabicy-clo [ 2,2,2 ]-octane, bis (trichlommethyl) carbonate. The reaction conditions were studied and seven inactive aromatic amine isothiocyanates were synthesized under the optimal conditions. The yield was up to 95％. Meanwhile, the structures were characterized by the infrared spectrum and NMR spectrum.关键词
异硫氰酸酯/不活泼芳胺/三乙烯二胺/双(三氯甲基)碳酸酯Key words
isothiocyanate/ inactive aromatic amine/ 1,4-diazabicyclo[ 2,2,2 ] -octane/ bis (trichloromethyl) carbonate分类
化学化工引用本文复制引用
蒋胜前,王周玉,蒋珍菊,陈万义,李建惠..不活泼芳胺异硫氰酸酯的合成研究[J].四川师范大学学报（自然科学版）,2011,34(3):388-391,4.基金项目
四川省青年基金(2010JQ0048)和四川省教育厅自然科学重点项目(09ZA110)基金资助项目 （2010JQ0048）
西华大学人才培养基金(R0720523)、西华大学研究生创新基金(YCJJ200942)和西华大学中药与生物技术校重点实验室对本文给予了资助 （R0720523）
