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正交试验法研究定形复合相变材料的制备工艺

张鸿 武晓华 王倩倩 王晓磊

大连工业大学学报2011,Vol.30Issue(3):199-202,4.
大连工业大学学报2011,Vol.30Issue(3):199-202,4.

正交试验法研究定形复合相变材料的制备工艺

Study on the preparation technology of composite phase change material by using orthogonal tests

张鸿 1武晓华 1王倩倩 1王晓磊1

作者信息

  • 1. 大连工业大学化工与材料学院,辽宁,大连,116034
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摘要

Abstract

In order to prepare shape-stabilized phase change material, composite phase change material was prepared by sol-gel. Shape material was obtained by sol-gel with TEOS, in which phase change material was auric acid/cetyl alcohol binary eutectic phase change materials. The results showed that the descending order of the influencing factors: ester-PCM ratio, ester-water ratio, pH, the reaction temperature, aging temperature. The best technology is: the ester-water ratio 1: 8, ester-PCM ratio 1 : 2.3, pH 3, aging temperature 85 ℃, the reaction temperature 60 ℃. When composite phase change material was prepared with the best technology, phase transition temperature of composite phase change material is 34 ℃, phase change enthalpy can reach 122.4 J/g when the mass fraction of phase change material is 64%.

关键词

溶胶-凝胶/相变材料/月桂酸/十六醇

Key words

sol-gel/ phase change material(PCM)/ lauric acid/ 16 alcohol

分类

通用工业技术

引用本文复制引用

张鸿,武晓华,王倩倩,王晓磊..正交试验法研究定形复合相变材料的制备工艺[J].大连工业大学学报,2011,30(3):199-202,4.

基金项目

大连市科技基金项目(2010J21DW014). (2010J21DW014)

大连工业大学学报

OA北大核心CSTPCD

1674-1404

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