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Fe3O4磁性纳米粒子-氧化石墨烯复合材料的可控制备及结构与性能表征

张燚 陈彪 杨祖培 张智军

物理化学学报2011,Vol.27Issue(5):1261-1266,6.
物理化学学报2011,Vol.27Issue(5):1261-1266,6.

Fe3O4磁性纳米粒子-氧化石墨烯复合材料的可控制备及结构与性能表征

Controlled Synthesis and Characterization of the Structure and Property of Fe3O4 Nanoparticle-Graphene Oxide Composites

张燚 1陈彪 2杨祖培 2张智军1

作者信息

  • 1. 陕西师范大学化学与材料科学学院,西安,710062
  • 2. 中国科学院苏州纳米技术与纳米仿生研究所,江苏,苏州,215123
  • 折叠

摘要

Abstract

Fe3O4 nanoparticle-graphene oxide (MGO) composites were prepared by chemically binding carboxylic acid-modified Fe3O4 nanoparticles to polyethylenimine-functionalized graphene oxide (GO).The structure, morphology, and magnetic properties of the composites were characterized by transmission electron microscopy (TEM), atomic force microscopy (AFM), X-ray diffraction (XRD), Fourier transform infrared (FT-IR) spectroscopy, thermogravimetric analysis (TGA), and vibrating sample magnetometry (VSM).The results show that the Fe3O4 nanoparticle content in the MGO composites can be easily controlled by changing the ratio of Fe3O4 nanoparticles to GO in the reaction mixture.The MGO composites obtained are superparamagnetic with high saturation magnetization, which can potentially be applied in magnetic targeted drug delivery, gene transport, magnetic resonance imaging, bioseparation, and magnetic guided removal of aromatic contaminants in waste water and in other fields.

关键词

氧化石墨烯/Fe3O4磁性纳米粒子/复合材料/可控制备/表征

Key words

Graphene oxide/ Fe3O4 nanoparticle/ Composite/ Controlled synthesis/ Characterization

分类

化学化工

引用本文复制引用

张燚 ,陈彪,杨祖培,张智军..Fe3O4磁性纳米粒子-氧化石墨烯复合材料的可控制备及结构与性能表征[J].物理化学学报,2011,27(5):1261-1266,6.

基金项目

国家自然科学基金(20873090,21073224)资助项目 (20873090,21073224)

物理化学学报

OA北大核心CSCDCSTPCDSCI

1000-6818

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