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香连胶囊的制备与质量标准研究

王薇 刘祖雄 覃贝 张连凤

中国药业2011,Vol.20Issue(13):29-30,2.
中国药业2011,Vol.20Issue(13):29-30,2.

香连胶囊的制备与质量标准研究

Preparation and Quality Control of Xianglian Capsule

王薇 1刘祖雄 1覃贝 1张连凤2

作者信息

  • 1. 中国人民解放军广州军区武汉总医院药剂科,湖北,武汉,430070
  • 2. 南昌大学医学院,江西,南昌,330038
  • 折叠

摘要

Abstract

Objective To study the preparation and quality control method of Xianglian Capsule. Methods Physic liquor were extracted by decoction and boil water method,and TLC was used for identification. HPLC was used to determine content of berberine hydrochloride. Results It can been checked the characteristic spot of Coptis chinensis and Radix Aucklandiae in the TLC , negative control have no interference. The calibration curves of berberine hydrochloride were linear within the range of 2. 0 - 80. 0 μg/mL( r = 0. 999 9); the average recovery rate was 100. 07% , RSD = 0. 41% ( n =9). Conclusion The preparation technology is reasonable , quality control method is feasible and reliable,the standard can provide a reference for the quality control of Xianglian Capsule.

关键词

香连胶囊/制备/质量标准/薄层色谱法/高效液相色谱法

Key words

Xianglian Capsule/ preparation/ berberine hydrochloride/ TLC: HPLC

分类

医药卫生

引用本文复制引用

王薇,刘祖雄,覃贝,张连凤..香连胶囊的制备与质量标准研究[J].中国药业,2011,20(13):29-30,2.

中国药业

OACSTPCD

1006-4931

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