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湿化学法制备多通道ZrO2超滤膜

周邢 邱鸣慧 范益群

南京工业大学学报(自然科学版)2011,Vol.33Issue(3):78-81,4.
南京工业大学学报(自然科学版)2011,Vol.33Issue(3):78-81,4.DOI:10.3969/j.issn.1671-7627.2011.03.017

湿化学法制备多通道ZrO2超滤膜

Preparation of multichannel Zr02 ultrafilration membrane with suspension derived from wet chemical synthesis

周邢 1邱鸣慧 1范益群1

作者信息

  • 1. 南京工业大学化学化工学院,材料化学工程国家重点实验室,江苏南京210009
  • 折叠

摘要

Abstract

Zirconia ultrafiltration membranes were fabricated by the wet chemical route.The multichannel zirconia mierofiltration membrane with the pore size of 200 nm served as the substrate, and zireonia nanoparticle suspension was used to form the membrane layer.The effects of sintering temperature on the microstrueture were investigated by X-ray diffraction (XRD) analysis and nitrogen adsorption/desorption.The morphology of the membrane was analyzed by scanning electron microscope (SEM).The permeation and separation performances of the membranes were evaluated by cross-section filtration.The results showed that the membranes were crack-free when the sintering temperature was controlled at 600 ℃.The membrane had higher pure water flux and the molecular weight cut off (MWCO) was 20 000 for multichannel zirconia membrane.The retention rate of the egg albumin (Mw =43 000) reached 95%.

关键词

陶瓷膜/超滤膜/烧结温度

Key words

ceramic membrane/ ultrafiltration membrane/ sintering temperature

分类

化学化工

引用本文复制引用

周邢,邱鸣慧,范益群..湿化学法制备多通道ZrO2超滤膜[J].南京工业大学学报(自然科学版),2011,33(3):78-81,4.

基金项目

国家重点基础研究发展计划(973计划)资助项目(2009CB623400) (973计划)

国家高技术研究发展计划(863 计划)资助项目(2007AA030303) (863 计划)

国家自然科学基金资助项目(20776067) (20776067)

南京工业大学学报(自然科学版)

OA北大核心CHSSCDCSTPCD

1671-7627

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