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Nb/SnO2复合薄膜的制备、结构及光电性能

曾乐贵 刘发民 钟文武 丁芃 蔡鲁刚 周传仓

物理学报2011,Vol.60Issue(3):779-784,6.
物理学报2011,Vol.60Issue(3):779-784,6.

Nb/SnO2复合薄膜的制备、结构及光电性能

Preparation and structure and optical-electrical properties of the Nb/SnO2 composite thin film

曾乐贵 1刘发民 2钟文武 1丁芃 1蔡鲁刚 1周传仓1

作者信息

  • 1. 北京航空航天大学物理科学与核能工程学院物理系纳米测控与低维物理教育部重点实验室,北京100191
  • 2. 装甲兵工程学院基础部,北京100072
  • 折叠

摘要

Abstract

The Nb/SnO2 composite thin films were successfully synthesized by sol-gel spin-coating method on glass substrate.The structures and properties of Nb/SnO2 composite thin films were characterized by X-ray diffraction ( XRD), scanning electron microscopey (SEM) , ultraviolet visible near-infrared spectrophotometry and four-probe method. The effects of Nb doping on structure and optical-electrical properties of the Nb/SnO2 composite thin films were researched. The results indicate that a tetragonal rutile structure is retained when the Nb content is less than 0.99at%, and the nano-particles are distributed homogeneously in the thin films and their size can be controlled in the range of 5-7 nm. The resistivity of Nb/SnO2 composite thin films decreases and then increases when the Nb content is less than 0.99at% , and reaches a very low value of 9.49 × 10-2 Ω·cm at 0.37at% Nb. In the range of 400-700 nm visible region, the transmittance of Nb/SnO2 composite thin films is up to 90% when the Nb content is less than 0.99at% , and the optical band gap of Nb/SnO2 composite thin films are in the range of 3.9-4.1 eV. The visible light transmittance of Nb/SnO2 composite thin films significantly reduce at 1.23at% Nb.

关键词

溶胶-凝胶法/Nb/SnO2复合薄膜/结构表征/光电性能

Key words

sol-gel/ Nb/SnO2 composite thin films/ structure characterization/ optical-electrical properties

引用本文复制引用

曾乐贵,刘发民,钟文武,丁芃,蔡鲁刚,周传仓..Nb/SnO2复合薄膜的制备、结构及光电性能[J].物理学报,2011,60(3):779-784,6.

基金项目

航天科学基金(批准号:373858)资助的课题. (批准号:373858)

物理学报

OA北大核心CSCDCSTPCD

1000-3290

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