农药学学报2011，Vol.13Issue(3)：293-298,6.DOI:10.3969/j.issn.1008-7303.2011.03.14
食品分析水平测试计划农药残留能力验证中分析方法的选择及其结果评价
Selection of the analytical methods and the results evaluation for the determination of pesticides residue in FAPAS proficiency tests
郏征伟 1苗水 1毛秀红 1陆继伟 1王柯 1季申1
作者信息
- 1. 上海市食品药品检验所,中药天然药物室,上海,201203
- 折叠
摘要
Abstract
Qualitative and quantitative analyses of pesticides residue in the samples of FAPAS (Food Analysis Performance Assessment Scheme) proficiency tests (PTs)were performed by identified and reliable analytical methods. Firstly, on-line chromatography and mass spectrometry was applied to screen the target compounds from a list of pesticides, and then the characteristics of the samples and the target compounds were evaluated in order to use an appropriate pre-processing technology and detection methods for quantitative analysis once the target pesticides were identified. The ｜Z｜ values of all the parameters in six FAPAS PTs were less than 2, and the results were satisfactory.关键词
食品分析水平测试计划/能力验证/农药/残留/分析/评价Key words
FAPAS/ proficiency test/ pesticide/ residue/ analysis/ evaluation分类
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郏征伟,苗水,毛秀红,陆继伟,王柯,季申..食品分析水平测试计划农药残留能力验证中分析方法的选择及其结果评价[J].农药学学报,2011,13(3):293-298,6.
