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离子色谱法检测饮用水中的草甘膦

刘玉欣 李锦 常凤启 卢振敏 王维榕

岩矿测试2011,Vol.30Issue(3):361-363,3.
岩矿测试2011,Vol.30Issue(3):361-363,3.

离子色谱法检测饮用水中的草甘膦

Determination of Glyphosate in Drinking Water by Ion Chromatography

刘玉欣 1李锦 1常凤启 1卢振敏 1王维榕1

作者信息

  • 1. 河北省疾病预防控制中心,河北石家庄,050021
  • 折叠

摘要

Abstract

A method for determination of glyphosate in water by ion chromatography was established in this paper. After removed residual chlorine by adding ascorbic acid and filtrated by micropore filtrer membrance, the water samples were directly injected into IC. The separation was carried out on IonPac ASI1-HC anion-exchange column and the eluent was 20 mmol/L KOH at flow rate of 1. 00 mL/min. The injection volume was 100 μL. The linearity of the method is from 0 to 1.5 mg/L. The detection limit was 0. 1 mg/L. The recoveries were from 95% to 106% , and RSD was from 5.08% to 7.09%. The experiments verified that the method was simple, sensitive, and accurate.

关键词

离子色谱法/草甘膦/饮用水

Key words

ion chromatography/ glyphosate/ drinking water

引用本文复制引用

刘玉欣,李锦,常凤启,卢振敏,王维榕..离子色谱法检测饮用水中的草甘膦[J].岩矿测试,2011,30(3):361-363,3.

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