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HPLC-ELSD法测定肾衰康口服液中黄芪甲苷的含量

石丽霞 张红岩 张振家

特产研究2011,Vol.33Issue(2):32-33,39,3.
特产研究2011,Vol.33Issue(2):32-33,39,3.

HPLC-ELSD法测定肾衰康口服液中黄芪甲苷的含量

Content Determination of Astraloside in Shenshuaikang Liquor by HPLC-ELSD

石丽霞 1张红岩 2张振家1

作者信息

  • 1. 吉林医药学院附属医院药剂科,吉林吉林132013
  • 2. 吉林省中医药科学院,长春130021
  • 折叠

摘要

Abstract

To determine the content of Astraloside in ShenShuaiKang Oral Liquor.Aatraloside in ShenShuaiKang Oral Liquor was determinated by HPLC-ELSD, Use the Diamonsil-C18 (4.6 × 250 mm,5 μ m) column, its mobile phase was acetenitrile-water (30:70).The flowrate was lmL/min, drift tube temperature was 105℃ ,and gas flow rate was 2.il.]min.It was showed that the Astraloside had a good linearity within the range of 0.4 μ g~4 μ g (r=0.999 5).The average recovery was 98.85 %, and RSD=I.65%(n=6).This method is simple and accurate for determination of Astraloside content in ShenShuaiKang Oral Liquor.

关键词

肾衰康口服液/黄芪甲苷/HPLC-ELSD法

Key words

Shenshuaikang oral liquor, Astraloside/ HPLC-ELSD

分类

生物科学

引用本文复制引用

石丽霞,张红岩,张振家..HPLC-ELSD法测定肾衰康口服液中黄芪甲苷的含量[J].特产研究,2011,33(2):32-33,39,3.

基金项目

吉林省教育厅"十一五"科学技术研究项目(2009-509) (2009-509)

特产研究

OACSTPCD

1001-4721

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