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麻黄"上沫"成分的热分析TG-DTG-DSC及热解-GC-MS研究

俞励平 梁晓亮 曾永长 罗佳波

中山大学学报(自然科学版)2011,Vol.50Issue(3):94-97,4.
中山大学学报(自然科学版)2011,Vol.50Issue(3):94-97,4.

麻黄"上沫"成分的热分析TG-DTG-DSC及热解-GC-MS研究

Ephedra Scum Components by Thermal TG-DTG-DSC Analysis and Pyrolytic GC-MS Analysis

俞励平 1梁晓亮 2曾永长 3罗佳波4

作者信息

  • 1. 南方医科大学中医药学院,广东广州510515
  • 2. 中山大学药物开发中心,广东广州510080
  • 3. 中国科学院广州地球化学研究所,广东广州510640
  • 4. 中国科学院研究生院,北京100049
  • 折叠

摘要

Abstract

The thermal properties of Ephedra scum was studied by TG-DTG and DSC methods while the components of Ephedra scum are further detected by pyrolytic GC-MS method.For Ephedra scum, the main temperature range of mass loss was 250 ~ 560 ℃.The fastest rate of mass loss was shown at 305 ℃ and 506.3 ℃.Two endothermic peaks were quite obvious respectively at 364.8 ℃ and 508.2 ℃.Ephedra scum is organic compound.The thermal decomposition product at 450 ℃ was analyzed by pyrolytic GC-MS, and twenty-eight chemical compounds were detected.

关键词

麻黄"上沫"/热分析/热解-GC-MS

Key words

Ephedra scum/ TG-DTG-DSC/ pyrolytic GC-MS

分类

医药卫生

引用本文复制引用

俞励平,梁晓亮,曾永长,罗佳波..麻黄"上沫"成分的热分析TG-DTG-DSC及热解-GC-MS研究[J].中山大学学报(自然科学版),2011,50(3):94-97,4.

基金项目

国家自然科学基金资助项目(30772756) (30772756)

中山大学学报(自然科学版)

OA北大核心CSCDCSTPCD

0529-6579

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