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n型Bi2Te3块体材料的放电等离子烧结及其性能研究

闫伟 江莞 王连军 张青红 李耀刚 王宏志

硅酸盐通报2011,Vol.30Issue(3):506-510,5.
硅酸盐通报2011,Vol.30Issue(3):506-510,5.

n型Bi2Te3块体材料的放电等离子烧结及其性能研究

Fabrication and Properties of n-type Bismuth Telluride Bulk Materials by SpaRk Plasma Sintering

闫伟 1江莞 2王连军 1张青红 2李耀刚 1王宏志1

作者信息

  • 1. 东华大学材料科学与工程学院,上海201620
  • 2. 中国科学院上海硅酸盐研究所,上海200050
  • 折叠

摘要

Abstract

n-type Bi2Te3 thermoelectric materials were prepared by spark plasma sintering method at 400 ℃, 420 ℃ and 440 ℃. The phase structure characterization of the samples were analyzed by X-ray diffraction pattern (XRD). The thermoelectric properties, including seebeck coefficient (a), electrical conductivity ( ó) and thermal conductivity (κ) were measured in the temperature range of 300-500 K. The MSP (Modified Small Punch) strength of n-type Bi2Te3 thermoelectric materials was discussed in detail. It was found that the maximum ZT value is about 0.79 of the sample sintered at 400 ℃, and the maximum MSP strength is about 119.5 MPa of the sample sintered at 440 ℃. It showed that MSP tests are reliable, convenient and efficient evaluation methods for ceramic materials by using quite small specimens.

关键词

碲化铋/放电等离子烧结/热电性能/力学性能

Key words

Bi2Te3/spark plasma sintering/ thermoelectric properties/ mechanical properties

分类

信息技术与安全科学

引用本文复制引用

闫伟,江莞,王连军,张青红,李耀刚,王宏志..n型Bi2Te3块体材料的放电等离子烧结及其性能研究 [J].硅酸盐通报,2011,30(3):506-510,5.

基金项目

国家863计划和中科院重大科研装备研制项目 ()

硅酸盐通报

OA北大核心CSCDCSTPCD

1001-1625

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