宁夏大学学报(自然科学版)2011,Vol.32Issue(2):151-153,3.
绿色溶剂乳酸乙酯下芳基醛亚胺的合成
Synthesis of Aryl Aidimines with A Green Solvent of Ethyl Lactate
摘要
Abstract
In order to promote the synthesis of aryl aldimines efficiently, the solvent system, ethyl lactate as a main solvent and the water as a polarity modifier, was investigated in the reaction of aromatic aldehyde and amine. The experimental results showed that in the presence of ethyl lactate and water solvent system, the products could be crystallized directly out of the solution within 0.2-60 minutes under the ambient condition in excellent yield of 85%-96% with no further purification. The synthetic method was easy-operational and eeo-friendly.关键词
乳酸乙酯/绿色溶剂/醛亚胺Key words
ethyl lactate/ green solvent/ aldimine分类
化学化工引用本文复制引用
谢婷,陈文华,徐景峰..绿色溶剂乳酸乙酯下芳基醛亚胺的合成[J].宁夏大学学报(自然科学版),2011,32(2):151-153,3.基金项目
江苏省自然科学基金资助项目(BK2010070) (BK2010070)