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流动注射化学发光法测定茶叶中的茶多酚

米娟 王九春 马永钧 刘彩云 周敏

宁夏大学学报(自然科学版)2011,Vol.32Issue(2):168-171,4.
宁夏大学学报(自然科学版)2011,Vol.32Issue(2):168-171,4.

流动注射化学发光法测定茶叶中的茶多酚

Determination of Tea Polyphenols in Tea Samples by Flow-Injection Chemiluminescence

米娟 1王九春 2马永钧 3刘彩云 1周敏2

作者信息

  • 1. 西北师范大学化学化工学院,甘肃兰州730070
  • 2. 西北师范大学肃省高分子材料重点实验室,甘肃兰州730070
  • 3. 西北师范大学省部共建生态环境相关高分子材料教育部重点实验室,甘肃兰州730070
  • 折叠

摘要

Abstract

A novel flow-injection chemiluminescence (FI-CL) for the determination of tea polyphenols was developed based on the chemiluminescence reaction of tea polyphenols in the galangin-potassium permanganatepolyphosphoric acid system. Under the optimized conditions, the obtained linear range was 1.0 × 10-8 - 5. 0 × 10-6 g/mL, with a detection limit of 2. 0 × 10-9 g/mL (3σ). The relative standard deviation (RSD) for the determination of 1.0×10-6 g/mL tea polyphenols was 2.0 % (n= 10). The proposed method has been used to determine the contents of tea polyphenols in Green tea, Black tea, Scented tea and Tie Guan Yin tea with recoveries in the range from 95.4% to 108. 3 %. The determination of tea polyphenols in tea samples by this method showed satisfactory results comparable with National Standard. It can be used for other phenolic compounds in food anahfsis and tesing.

关键词

流动注射/化学发光/高良姜素/高锰酸钾/茶多酚

Key words

flow-injection/ chemiluminescence/ galangin/ potassium permanganate/ tea polyphenols

分类

化学化工

引用本文复制引用

米娟,王九春,马永钧,刘彩云,周敏..流动注射化学发光法测定茶叶中的茶多酚[J].宁夏大学学报(自然科学版),2011,32(2):168-171,4.

基金项目

甘肃省自然科学基金资助项目(1010RJZA017) (1010RJZA017)

宁夏大学学报(自然科学版)

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