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一种改进的水产品中硝基呋喃代谢物测定方法研究

梁剑 朱品玲 钟茂生 陈舒奕

安徽农业科学2009,Vol.37Issue(33):16198-16199,16212,3.
安徽农业科学2009,Vol.37Issue(33):16198-16199,16212,3.

一种改进的水产品中硝基呋喃代谢物测定方法研究

Study on A Modified Method of Extracting Nitrofuran Metabolites in Fishery Product

梁剑 1朱品玲 1钟茂生 1陈舒奕1

作者信息

  • 1. 中华人民共和国宁德出入境检验检疫局,福建宁德,352100
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摘要

Abstract

Based on referring to the government standard and industry standards (SN/T 1627-2005), the detection method of nitrofuran metabolites in fishery products was explored by using LC/MS. It can remove the interference of pre-processing using substance to make recovery quantization. From chromatograms of LC/MS, it was shown that the detection of nitrofuran metabolites reached good effect. As for the recovery curve, nitrofuran metabolites added standard curve reached better linear relation. The detection limits of melamine in the muscle tissue of water products using LC/MS were 0.5 μg/kg.

关键词

液相色谱质谱联用仪/硝基呋喃代谢物/水产品

Key words

Liquid chromatography/Mass spectrometer/ Nitrofuran metabolites/ Fishery products

分类

轻工纺织

引用本文复制引用

梁剑,朱品玲,钟茂生,陈舒奕..一种改进的水产品中硝基呋喃代谢物测定方法研究[J].安徽农业科学,2009,37(33):16198-16199,16212,3.

安徽农业科学

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